Bibenzyl hydroperoxide synthesis
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United States of America Patent
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Apr 1, 1986
Grant Date -
N/A
app pub date -
Nov 13, 1984
filing date -
Nov 13, 1984
priority date (Note) -
Expired
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Abstract
Substantially quantitative yields of bibenzyl hydroperoxide and bibenzyl dihydroperoxide can be obtained when oxygen is reacted with bibenzyl (1,2-diphenylethane) in the presence of a minor amount of sodium bicarbonate at a temperature within the range of about 100.degree. to about 160.degree. C. to provide an oxidation product wherein the bibenzyl is substantially selectively converted to the bibenzyl hydroperoxides. The bibenzyl hydroperoxides can be used as raw materials for the production of propylene oxide by reacting the bibenzyl hydroperoxides with propylene.
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